化工社化工社 化学情報印刷レポート · 研究参考用
3,5-Dibromosalicylaldehyde → HCID 178449914、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 3,5-Dibromosalicylaldehyde | HCID 7024 | — |
| 反応物 | N-tert-butylhydroxylamine | HCID 98586 | — |
| 生成物 | HCID 178449914 | HCID 178449914 | — |
反応手順
The title compound was prepared according to the procedure described in Example 13 using 3,5-dibromo-2-hydroxybenzaldehyde and N-tert-butylhydroxylamine. The title compound was isolated in 68.7% yield as a yellow crystalline solid, m.p. 111.3° C. (Rf=0.54 on a silica gel plate using 7:3 hexanes/EtOAc as an eluant).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06197826B1 |
| 出典データセット | uspto-grants-2001_03 |
| ORD ID | ord-5175da832f654f48a85633dbe044f612 |
| 出典メモ | uspto-grants-2001_03 |