化工社化工社 化学情報印刷レポート · 研究参考用
5-Bromosalicylaldehyde → HCID 178449915、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 5-Bromosalicylaldehyde | HCID 72863 | — |
| 反応物 | N-tert-butylhydroxylamine | HCID 98586 | — |
| 生成物 | HCID 178449915 | HCID 178449915 | — |
反応手順
The title compound was prepared according to the procedure described in Example 1 using 5-bromo-2-hydroxybenzaldehyde and N-tert-butylhydroxylamine. The title compound was isolated in 68.7% yield as a yellow crystalline solid, m.p. 118.7° C. (Rf=0.65 on a silica gel plate using 1:1 EtOAc/hexanes as an eluant).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06197826B1 |
| 出典データセット | uspto-grants-2001_03 |
| ORD ID | ord-de7a2748ebe648fd8b933d3c61c58394 |
| 出典メモ | uspto-grants-2001_03 |