関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Aniline | HCID 6115 | — |
| 反応物 | Sodium hydride | HCID 24758 | — |
| 反応物 | 1,2,3-Trimethylcyclopentadiene | HCID 138063 | — |
| 溶媒 | Tetrahydrofuran | HCID 8028 | — |
| 生成物 | HCID 178425477 | HCID 178425477 | — |
反応手順
Sodium hydride (containing mineral oil; the content of sodium hydride: 60%) (0.80 g) and aniline (0.046 g) were added to the solution of trimethylcyclopentadiene (1.08 g) dissolved in tetrahydrofuran (6.12 g), and stirred at 50° C. for 3 hours. Thus, trimethylcyclopentadienylsodium was obtained in the form of a solution in tetrahydrofuran.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US06197990B1 |
|---|
| 出典データセット | uspto-grants-2001_03 |
|---|
| ORD ID | ord-be34fdff6d8d4ce9a642a171482e678f |
|---|
| 出典メモ | uspto-grants-2001_03 |
|---|
