化工社化工社 化学情報印刷レポート · 研究参考用
Ethyl bromoacetate → 2-[3-Hydroxy-5-[hydroxymethyl]phenyloxy]acetic acid, ethyl ester
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Ethyl bromoacetate | HCID 7748 | — |
| 反応物 | 3,5-Dihydroxybenzyl alcohol | HCID 34661 | — |
| 生成物 | 2-[3-Hydroxy-5-[hydroxymethyl]phenyloxy]acetic acid, ethyl ester | HCID 121006484 | — |
反応手順
the subtitle compound was prepared from 3,5-dihydroxybenzyl alcohol (5 g) and ethyl bromoacetate (5.96 g) by the method of example 21 step (ii). Purified by chromatography eluting with 30% ethyl acetate in isohexane. Yield 1.6 g.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06200981B1 |
| 出典データセット | uspto-grants-2001_03 |
| ORD ID | ord-73387faa66d54a03a2d15275ebeac7c2 |
| 出典メモ | uspto-grants-2001_03 |