HCID 9801871、化合物 → HCID 9824989、化合物

HRID 1532643ノート

反応式

HRID 1532643 の反応式
[ClH:1].C(OCC)(=O)C.[CH3:8][N:9]([CH3:37])[CH2:10][CH2:11][CH2:12][N:13]1[C:17]2[CH:18]=[CH:19][CH:20]=[CH:21][C:16]=2[N:15]=[C:14]1[CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH2:29][CH2:30][CH2:31][CH2:32][CH2:33][CH2:34][CH2:35][CH3:36]>C(OCC)(=O)C>[ClH:1].[CH3:37][N:9]([CH3:8])[CH2:10][CH2:11][CH2:12][N:13]1[C:17]2[CH:18]=[CH:19][CH:20]=[CH:21][C:16]=2[N:15]=[C:14]1[CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH2:29][CH2:30][CH2:31][CH2:32][CH2:33][CH2:34][CH2:35][CH3:36]

参加物

4

反応物 2

HCID 9801871HCID 9801871、化合物HCID 21866389Hydrogen chloride-ethyl acetate

生成物 1

HCID 9824989HCID 9824989、化合物

試薬・触媒・溶媒 1

HCID 8857Ethyl Acetate溶媒

実験手順

4N Hydrochloric acid/ethyl acetate solution (0.13 ml) was added to a solution containing N,N-dimethyl-3-(2-pentadecyl-1H-benzimidazol-1-yl)-1-propanamine (0.20 g) in ethyl acetate (2 ml). After being stirred for 20 minutes at room temperature, the reaction mixture was concentrated. The residue was recrystallized with the mixed solution of ethyl acetate-hexane, thereby yielding the entitled compound (0.13 g) as white solid.

後処理

  1. concentrationthe reaction mixture was concentrated
  2. customThe residue was recrystallized with the mixed solution of ethyl acetate-hexane

出典と根拠

ORDレコード
ord-20e82b5fab2649ee80729924cb92e72e
出典データセット
uspto-grants-2001_03
特許番号
US06204264B1

反応ノート

読み込み中…