Isopropanol → 2,3,3,4,4-Pentafluorocyclobutenyl isopropyl ether

HRID 1534276

反応式

HRID 1534276 の反応式
[OH-].[K+].F[C:4]1[C:7]([F:9])([F:8])[C:6]([F:11])([F:10])[C:5]=1[F:12].[CH:13]([OH:16])([CH3:15])[CH3:14]>C(OCC)C>[CH:13]([O:16][C:4]1[C:7]([F:8])([F:9])[C:6]([F:10])([F:11])[C:5]=1[F:12])([CH3:15])[CH3:14]

参加物

5

反応物 3

HCID 3776IsopropanolHCID 12767HexafluorocyclobuteneHCID 14797Potassium Hydroxide

生成物 1

HCID 199110612,3,3,4,4-Pentafluorocyclobutenyl isopropyl ether

試薬・触媒・溶媒 1

HCID 3283Diethyl Ether溶媒

実験手順

70 g (1.23 mol) of powdered potassium hydroxide are metered into a solution of 200 g (1.23 mol) of 1,2,3,3,4,4-hexafluorocyclobutene and 90 g (1:5 mol) of isopropanol in 800 ml of diethyl ether at room temperature. The mixture is stirred for a further hour and worked up as described in Example 1. The product is then distilled.

後処理

  1. distillationThe product is then distilled

出典と根拠

ORDレコード
ord-bfef5c94b8544c07810aa926c21820e5
出典データセット
uspto-grants-1992_02
特許番号
US05087775

関連ノート

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