Methanesulfonic Acid → HCID 13131214、化合物

HRID 1534633ノート

反応式

HRID 1534633 の反応式
O[CH2:2][C:3]([NH:6][C:7]([CH3:12])([CH2:10][CH3:11])[CH2:8][OH:9])([CH3:5])[CH3:4].CS(O)(=O)=O>>[CH3:12][C:7]1([CH2:10][CH3:11])[CH2:8][O:9][CH2:2][C:3]([CH3:5])([CH3:4])[NH:6]1

参加物

4

反応物 2

HCID 6395Methanesulfonic AcidHCID 131312092-[(1-Hydroxy-2-methylpropan-2-yl)amino]-2-methylbutan-1-ol

生成物 1

HCID 13131214HCID 13131214、化合物収率 50%

試薬・触媒・溶媒 1

HCID 178435178HCID 178435178、化合物溶媒

実験手順

In a manner analogous to that described in example 5A hereinabove, starting with (1-hydroxy-2-methyl-2-propyl)(1-hydroxy-2-methyl-2-butyl)amine and reacting with methanesulfonic acid, then working up the reaction mixture, a colorless oil having a bp 71°-3° C./20 mm, is obtained in about 50% yield. Less than 5% by weight of the oil is found to provide excellent u-v light stability in polypropylene.

後処理

  1. customis obtained in about 50% yield

出典と根拠

ORDレコード
ord-7bc5bbe50ee343a3a32f6eb654d0bd53
出典データセット
uspto-grants-1992_02
特許番号
US05089614

反応ノート

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