Hydrochloric Acid → HCID 19908400、化合物

HRID 1534844ノート

反応式

HRID 1534844 の反応式
[O-:1][C:2]#[N:3].[K+].[C:5]([NH:10][NH2:11])([CH2:8][CH3:9])([CH3:7])[CH3:6].Cl>O>[C:5]([NH:10][NH:11][C:2]([NH2:3])=[O:1])([CH2:8][CH3:9])([CH3:7])[CH3:6]

参加物

5

反応物 3

HCID 313Hydrochloric AcidHCID 117546HCID 117546、化合物HCID 11378442Potassium cyanate

生成物 1

HCID 19908400HCID 19908400、化合物

試薬・触媒・溶媒 1

HCID 962Water溶媒

実験手順

13.6 g of potassium cyanate are added to a mixture of 17 g of tert-pentylhydrazine and 30 ml of water cooled in an ice bath and 16.5 g of conc. hydrochloric acid are then added dropwise. The mixture is stirred at room temperature for 3 h and the solid is filtered off with suction, washed with water and dried in vacuo.

後処理

  1. temperaturecooled in an ice bath
  2. filtrationthe solid is filtered off with suction
  3. washwashed with water
  4. customdried in vacuo

出典と根拠

ORDレコード
ord-4d8ee08daba343dfb7c4cd34613a8364
出典データセット
uspto-grants-1992_02
特許番号
US05091398

反応ノート

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