化工社化工社 化学情報印刷レポート · 研究参考用
4-Chlorobenzenesulfonyl chloride → Benzyl(4-chlorobenzenesulfonyloxymethyl)phosphinic acid, n-butyl ester
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 4-Chlorobenzenesulfonyl chloride | HCID 7398 | — |
| 反応物 | Benzylhydroxymethylphosphinic acid, n-butyl ester | HCID 86752201 | — |
| 生成物 | Benzyl(4-chlorobenzenesulfonyloxymethyl)phosphinic acid, n-butyl ester | HCID 86752202 | — |
反応手順
The title compound was prepared from benzylhydroxymethylphosphinic acid, n-butyl ester and 4-chlorobenzenesulfonyl chloride according to the method described in Procedure 32. The resulting white solid (mp 87°-88° C.) was used in the next stage without further purification.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05726165 |
| 出典データセット | uspto-grants-1998_03 |
| ORD ID | ord-1b2ca7107578479d93f1b4ae6d8fd313 |
| 出典メモ | uspto-grants-1998_03 |