関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | O-Xylene | HCID 7237 | — |
| 反応物 | 2-Nitroamino-2-imidazoline | HCID 410042 | — |
| 反応物 | 2-Amino-1-(4-methylphenyl)ethan-1-ol | HCID 3519929 | — |
| 溶媒 | Acetone | HCID 180 | — |
| 生成物 | alpha-(2-Imidazolin-2-ylaminomethyl)-p-methylbenzyl alcohol | HCID 53928717 | — |
反応手順
A mixture of 9.06 parts of α-(aminomethyl)-p-methylbenzyl alcohol, 7.8 parts of 2-(nitramino)-2-imidazoline and 8 parts of xylene is stirred for 30 minutes at 160°C (oil-bath). The reaction mixture is cooled and acetone is added. The precipitated product is filtered off, washed with acetone and dried, yielding α-(2-imidazolin-2-ylaminomethyl)-p-methylbenzyl alcohol; 163.7°C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US03983133 |
|---|
| 出典データセット | uspto-grants-1976_09 |
|---|
| ORD ID | ord-c621f94f9ce7425795b4c019eb926d30 |
|---|
| 出典メモ | uspto-grants-1976_09 |
|---|
