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3-(4-Methoxyphenyl)-1-phenylprop-2-en-1-one → 8-(4-Methoxyphenyl)-10,10-dimethyl-6-phenyl-10H-pyrido[1,2-a]indolium perchlorate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 3-(4-Methoxyphenyl)-1-phenylprop-2-en-1-one | HCID 94197 | — |
| 反応物 | 3H-Indole, 2,3,3-trimethyl-, perchlorate | HCID 14913188 | — |
| 生成物 | 8-(4-Methoxyphenyl)-10,10-dimethyl-6-phenyl-10H-pyrido[1,2-a]indolium perchlorate | HCID 12374370 | — |
反応手順
2,3,3-Trimethyl-3H-indolium perchlorate (5 g.) and 3-(4-methoxyphenyl)-1-phenyl-prop-2-ene-1-one (10 g.) were heated together on a steam bath for three hours. The cooled mixture was purified by recrystallization from acetonitrile. The melting point is 258°C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US03983288 |
| 出典データセット | uspto-grants-1976_09 |
| ORD ID | ord-a47521511e23444a9257f90a109acb4d |
| 出典メモ | uspto-grants-1976_09 |