N,N'-Dimethylurea → HCID 178483127、化合物
反応式
[C:1]([C:9]1[S:13][C:12]2[CH:14]=[CH:15][CH:16]=[CH:17][C:11]=2[C:10]=1[OH:18])(=O)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[CH3:19][NH:20]C(NC)=O>C(OCC)(=O)C>[CH3:19][NH:20]/[C:1](/[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1)=[C:9]1\[C:10](=[O:18])[C:11]2[CH:17]=[CH:16][CH:15]=[CH:14][C:12]=2[S:13]\1参加物
4
実験手順
Prepared as in Example 31 from 2-benzoyl-benzo[b]thiophen-3-ol, but using N,N'-dimethylurea in place of ammonium acetate, with a yield of 66% of theory, m.p. 156°-157° C. (ethyl acetate). On the basis of its thin-layer chromatogram, mixed melting point, elemental analysis and IR spectrum, the product was identical to that of Example 2.
後処理
- additionOn the basis of its thin-layer chromatogram, mixed
出典と根拠
- ORDレコード
- ord-143478e5b90d4374b0cad7f3d23db77f
- 出典データセット
- uspto-grants-1981_09
- 特許番号
- US04288437
反応ノート
読み込み中…