Hydrochloric Acid → Sulfanilamide Hydrochloric Acid Brij 35

HRID 1578220ノート

反応式

HRID 1578220 の反応式
[S:1]([NH2:11])(=[O:10])([C:3]1[CH:8]=[CH:7][C:6]([NH2:9])=[CH:5][CH:4]=1)=[O:2].[CH3:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][O:24][CH2:25][CH2:26][OH:27].[ClH:28]>O>[S:1]([NH2:11])(=[O:10])([C:3]1[CH:4]=[CH:5][C:6]([NH2:9])=[CH:7][CH:8]=1)=[O:2].[ClH:28].[CH3:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][O:24][CH2:25][CH2:26][OH:27]

参加物

5

反応物 3

HCID 313Hydrochloric AcidHCID 5333Sulfanilamide2 回HCID 247502-(Dodecyloxy)ethanol

生成物 1

HCID 131712428Sulfanilamide Hydrochloric Acid Brij 35

試薬・触媒・溶媒 1

HCID 962Water溶媒2 回

実験手順

To a 2 liter volumetric flask containing approximately 1500 ml. of distilled water is added 20.0 g. of sulfanilamide (0.116 mol), 66 ml. of Brij 35 and 200 ml. of concentrated hydrochloric acid. The resulting mixture is taken up to 2 liters with distilled water and then stirred until the sulfanilamide is completely dissolved.

後処理

  1. additionTo a 2 liter volumetric flask containing approximately 1500 ml
  2. dissolutionis completely dissolved

出典と根拠

ORDレコード
ord-5bde5d665a8e41d9bcf7e6b78f5c52a5
出典データセット
uspto-grants-1981_09
特許番号
US04292040

反応ノート

読み込み中…