1,2,3,6-Tetrahydro-4-phenylpyridine → HCID 21559978、化合物
反応式
[C:1]([N:4]1[C:12]2[CH:11]=[C:10]3[O:13][CH2:14][O:15][C:9]3=[CH:8][C:7]=2[CH:6]([CH2:16][CH2:17]Br)[CH2:5]1)(=[O:3])[CH3:2].[C:19]1([C:25]2[CH2:26][CH2:27][NH:28][CH2:29][CH:30]=2)[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=1>>[C:1]([N:4]1[C:12]2[CH:11]=[C:10]3[O:13][CH2:14][O:15][C:9]3=[CH:8][C:7]=2[CH:6]([CH2:16][CH2:17][N:28]2[CH2:27][CH:26]=[C:25]([C:19]3[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=3)[CH2:30][CH2:29]2)[CH2:5]1)(=[O:3])[CH3:2]参加物
3
実験手順
In the manner described in Example 1, treatment of 5-acetyl-7-(2-bromoethyl)-6,7-dihydro-5H-1,3-dioxolo[4,5-f]-indole with 1,2,3,6-tetrahydro-4-phenylpyridine gives white crystals, m.p. 90°-91°C., after recrystallization from dilute acetone.
後処理
- customgives white crystals, m.p. 90°-91°C.
- customafter recrystallization from dilute acetone
出典と根拠
- ORDレコード
- ord-364f9cf2efbe444dbd4afad4363b7127
- 出典データセット
- uspto-grants-1976_02