化工社化工社 化学情報印刷レポート · 研究参考用
Oxygen → Trioctyl phosphate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Oxygen | HCID 977 | — |
| 反応物 | Octyl phosphite | HCID 76413 | — |
| 触媒 | Cobalt octoate | HCID 8696 | — |
| 生成物 | Trioctyl phosphate | HCID 15733 | 91% |
反応手順
A mixture of 0.2 g. of cobalt octoate and 70 g. of trioctyl phosphite is warmed in vacuo (10 mm.) at 30°C while oxygen is added over a period of six hours. The mixture is stirred throughout this period by means of a magnetic stirrer. The product is washed with an aqueous alkaline solution to remove the cobalt catalyst, having a 91% yield of trioctyl phosphate.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US03939229 |
| 出典データセット | uspto-grants-1976_02 |
| ORD ID | ord-872a2dab69c84d7d96c8950da038a833 |
| 出典メモ | uspto-grants-1976_02 |