Hydrogen iodide → HCID 21567192、化合物

反応式

CC1N=CC2C(C=1)=C([N+]([O-])=O)C=CC=2.[Cl:15][C:16]1[CH:25]=[CH:24][C:23]([N+:26]([O-:28])=[O:27])=[C:22]2[C:17]=1[CH:18]=[CH:19][N:20]=[CH:21]2.Cl.CC1N=CC2C(C=1)=C([N+]([O-])=O)C=CC=2.[IH:44]>>[IH:44].[Cl:15][C:16]1[CH:25]=[CH:24][C:23]([N+:26]([O-:28])=[O:27])=[C:22]2[C:17]=1[CH:18]=[CH:19][N:20]=[CH:21]2

参加物

反応物 4

HCID 24841Hydrogen iodide

HCID 2749733-Methyl-5-nitroisoquinoline

HCID 3180535-CHLORO-8-NITROISOQUINOLINE

HCID 21567166HCID 21567166、化合物

生成物 1

HCID 21567192HCID 21567192、化合物

実験手順

was prepared by the procedure of Example 11 hereinabove, except that the 3-methyl-5-nitro-isoquinoline of that example was replaced by 5-chloro-8-nitro-isoquinoline, and the concentrated hydrochloric acid of Example 11 was replaced by concentrated hydriodic acid, to yield 5-chloro-8-nitro-isoquinoline hydro-iodide, melting over the range 161°-5°C.