7-Hydrazino-2,3dihydro-2-methylbenzofuran → HCID 13535833、化合物

HRID 1583755ノート

反応式

HRID 1583755 の反応式
[NH:1]([C:3]1[C:11]2[O:10][C:9]([CH3:13])([CH3:12])[CH2:8][C:7]=2[C:6]([CH3:14])=[CH:5][CH:4]=1)[NH2:2].ClC(N(C1C2OC(C)CC=2C=CC=1)N[C:20]([N:22]([O:24][CH3:25])[CH3:23])=[O:21])=O.N(C1C2[O:45][CH:44](C)CC=2C=CC=1)N>>[CH3:13][C:9]1([CH3:12])[CH2:8][C:7]2[C:6]([CH3:14])=[CH:5][CH:4]=[C:3]([N:1]3[N:2]=[C:20]([N:22]([O:24][CH3:25])[CH3:23])[O:21][C:44]3=[O:45])[C:11]=2[O:10]1

参加物

4

反応物 3

HCID 135358277-Hydrazino-2,3dihydro-2-methylbenzofuranHCID 13535829HCID 13535829、化合物HCID 135358327-Hydrazino-2,3-dihydro-2,2,4-trimethylbenzofuran

生成物 1

HCID 13535833HCID 13535833、化合物

実験手順

3 was prepared, as an amber syrup, by treating 7-hydrazino-2,3-dihydro-2,2,4-trimethylbenzofuran (prepared by the method described in U.S. Pat. No. 4,406,910) according to the procedures described in Example 1 for preparing 1F from 1D.

後処理

  1. custom3 was prepared, as an amber syrup
  2. customprepared by the method

出典と根拠

ORDレコード
ord-9204112cd66d4dc1b52b03905c5cbf11
出典データセット
uspto-grants-1985_11
特許番号
US04554283

反応ノート

読み込み中…