化工社化工社 化学情報印刷レポート · 研究参考用
2-Ethylbutyraldehyde → 3,7-Diethyl-5-azanona-3,5-diene
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2-Ethylbutyraldehyde | HCID 7359 | — |
| 反応物 | Ammonium Hydroxide | HCID 14923 | — |
| 生成物 | 3,7-Diethyl-5-azanona-3,5-diene | HCID 12413470 | 76.5% |
反応手順
To a sample of 250 grams of 28% ammonium hydroxide was added 215 grams of 2-ethylbutyraldehyde and the heterogeneous mixture was stirred for 18 hours at ambient temperature. The resulting organic layer was separated, and after drying, slowly distilled at atmospheric pressure to yield 148.8 grams of 3,7-diethyl-5-azanona-3,5-diene. Mass spectrum m/e=181. 13C nuclear magnetic resonance spectrum, solvent CDCl3, ref. TMS. ##STR7##
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04555576 |
| 出典データセット | uspto-grants-1985_11 |
| ORD ID | ord-546100d3352a4001a06fac0ff0155d98 |
| 出典メモ | uspto-grants-1985_11 |