化工社化工社 化学情報印刷レポート · 研究参考用
2-Methylimidazole → 1-((6-chloro-1,3-benzodioxol-5-yl)methyl)2-methyl-1H-imidazole
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2-Methylimidazole | HCID 12749 | — |
| 反応物 | Sodium hydride | HCID 24758 | — |
| 反応物 | 6-Chloropiperonyl chloride | HCID 90113 | — |
| 溶媒 | Dimethylformamide | HCID 6228 | — |
| 生成物 | 1-((6-chloro-1,3-benzodioxol-5-yl)methyl)2-methyl-1H-imidazole | HCID 21224807 | — |
反応手順
The operation is carried out as in Stage 1 of Example 11 starting with 12.3 g of 2-methyl-1H-imidazole, 7.92 g of sodium hydride with 50% oil, 150 ml of N dimethylformamide and 33.8 g of 6-chloropiperonyl chloride.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05932741 |
| 出典データセット | uspto-grants-1999_08 |
| ORD ID | ord-6b398965cfb84cc889a194adca6f3e3c |
| 出典メモ | uspto-grants-1999_08 |