3,5-Dimethyl-4-hydroxybenzaldehyde → (E)-3-(3,5-Dimethyl-4-hydroxyphenyl)2-[(3-phenyl-n-propyl)aminosulfonyl]acrylonitrile

反応式

[CH3:1][C:2]1[CH:3]=[C:4]([CH:7]=[C:8]([CH3:11])[C:9]=1[OH:10])[CH:5]=O.[C:12]1([CH2:18][CH2:19][CH2:20][NH:21][S:22]([CH2:25][C:26]#[N:27])(=[O:24])=[O:23])[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1>>[CH3:1][C:2]1[CH:3]=[C:4](/[CH:5]=[C:25](/[S:22]([NH:21][CH2:20][CH2:19][CH2:18][C:12]2[CH:13]=[CH:14][CH:15]=[CH:16][CH:17]=2)(=[O:24])=[O:23])\[C:26]#[N:27])[CH:7]=[C:8]([CH3:11])[C:9]=1[OH:10]

参加物

反応物 2

HCID 752223,5-Dimethyl-4-hydroxybenzaldehyde

HCID 15410494(3-Phenyl-n-propyl)aminosulfonylacetonitrile

生成物 1

HCID 15516465(E)-3-(3,5-Dimethyl-4-hydroxyphenyl)2-[(3-phenyl-n-propyl)aminosulfonyl]acrylonitrile

実験手順

The titled compound was prepared with 3,5-dimethyl-4-hydroxybenzaldehyde and N-3-phenyl-n-propyl cyanomethylsulfonamide under the similar conditions as described for EXAMPLE 12 (part B).

出典と根拠

ORDレコード: ord-69a28317e1194c04bb9cc687ddeb7616
出典データセット: uspto-grants-1999_08
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US05935993

反応ノート

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