Methanol → 3-Methyl-1-(2-piperidinophenyl)-1-butylamine, (S)-
反応式
[CH3:1][CH:2]([CH3:18])[CH2:3][CH:4]([NH2:17])[C:5]1[CH:10]=[CH:9][CH:8]=[CH:7][C:6]=1[N:11]1[CH2:16][CH2:15][CH2:14][CH2:13][CH2:12]1.C(N[C@H](C(O)=O)CCC(O)=O)(=O)C.CO>CC(C)=O>[CH3:1][CH:2]([CH3:18])[CH2:3][C@H:4]([NH2:17])[C:5]1[CH:10]=[CH:9][CH:8]=[CH:7][C:6]=1[N:11]1[CH2:16][CH2:15][CH2:14][CH2:13][CH2:12]1参加物
5
実験手順
Equimolar quantities of racemic 3-methyl-1-(2-piperidino-phenyl)-1-butylamine and of N-acetyl-L-glutamic acid were refluxed in aceton, whereby methanol was added in such an amount to yield a clear solution.
後処理
- customto yield a clear solution
出典と根拠
- ORDレコード
- ord-87c5e5558fd54e07848bb08cd8904b15
- 出典データセット
- uspto-grants-1993_06
- 特許番号
- US05216167
反応ノート
読み込み中…