Methanesulfonyl chloride → 2-{3-[(Methylsulfonyl)amino]phenyl}ethyl methanesulfonate

HRID 15873

反応式

HRID 15873 の反応式
[NH2:1][C:2]1[CH:3]=[C:4]([CH:8]=[CH:9][CH:10]=1)[CH2:5][CH2:6][OH:7].[CH3:11][S:12](Cl)(=[O:14])=[O:13]>>[CH3:11][S:12]([O:7][CH2:6][CH2:5][C:4]1[CH:8]=[CH:9][CH:10]=[C:2]([NH:1][S:12]([CH3:11])(=[O:14])=[O:13])[CH:3]=1)(=[O:14])=[O:13]

参加物

3

反応物 2

HCID 31297Methanesulfonyl chlorideHCID 149389872-(3-Aminophenyl)ethan-1-ol

生成物 1

HCID 574443592-{3-[(Methylsulfonyl)amino]phenyl}ethyl methanesulfonate

実験手順

The title compound was prepared from 3-aminophenethyl alcohol (U.S. Pat. No. 2,641,602) and methanesulfonyl chloride (2 eq.) according to the procedure contained within description 4. The product was used immediately without further purification or characterisation.

後処理

  1. customThe product was used immediately without further purification or characterisation

出典と根拠

ORDレコード
ord-df39bbbc55b94cc4a4671516af5755d6
出典データセット
uspto-grants-2010_06
特許番号
US07732600B2

関連ノート

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