Triethylamine → Cobalt octoate

HRID 1588081

反応式

HRID 1588081 の反応式
[CH2:1](N(CC)CC)[CH3:2].C([CH:10]([CH2:15][CH2:16][CH2:17]C)[CH2:11][C:12]([OH:14])=[O:13])C.[N+]([O-])([O-])=O.[Co+2:23].[N+]([O-])([O-])=O>C1CCCCC1>[CH3:17][CH2:16][CH2:15][CH2:10][CH:11]([C:12]([O-:14])=[O:13])[CH2:1][CH3:2].[CH3:17][CH2:16][CH2:15][CH2:10][CH:11]([C:12]([O-:14])=[O:13])[CH2:1][CH3:2].[Co+2:23]

参加物

5

反応物 3

HCID 8471TriethylamineHCID 25000Cobalt dinitrateHCID 1397153-Ethylheptanoic acid

生成物 1

HCID 8696Cobalt octoate収率 55.5%

試薬・触媒・溶媒 1

HCID 8078Cyclohexane溶媒

実験手順

Using a 1 liter flask, 0.40 mol triethylamine is added with stirring at room temperature to 0.40 mol 2-ethyl hexane carboxylic acid. After the exothermic reaction has abated, the reaction mixture is diluted with 65 ml cyclohexane and 0.20 mol cobalt nitrate is added. After stirring for 30 minutes, the reaction solution is filtered, leaving a 55.5% blue cobalt octoate solution in cyclohexane.

後処理

  1. customAfter the exothermic reaction
  2. additionis added
  3. filtrationthe reaction solution is filtered

出典と根拠

ORDレコード
ord-ae8fdf9f837b4f1f9f9691ad0a891fb6
出典データセット
uspto-grants-1993_06
特許番号
US05220045

関連ノート

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