Beta-Aminobutyric Acid → HCID 70072142、化合物

HRID 1588092ノート

反応式

HRID 1588092 の反応式
[C:1]([C:3]1[CH:8]=[CH:7][C:6]([CH2:9][CH2:10][CH2:11][CH2:12][C:13]([OH:15])=O)=[CH:5][CH:4]=1)#[N:2].[CH3:16][CH:17]([CH2:19][C:20]([OH:22])=[O:21])[NH2:18].C1(C(CC(O)=O)[NH2:30])C=CC=CC=1>>[NH2:30][N:2]=[CH:1][C:3]1[CH:4]=[CH:5][C:6]([C:9]#[C:10][CH2:11][CH2:12][C:13]([NH:18][CH:17]([CH3:16])[CH2:19][C:20]([OH:22])=[O:21])=[O:15])=[CH:7][CH:8]=1

参加物

4

反応物 3

HCID 10932Beta-Aminobutyric AcidHCID 69189DL-beta-PhenylalanineHCID 152807295-(4-Cyanophenyl)pentanoic acid

生成物 1

HCID 70072142HCID 70072142、化合物

実験手順

The title compound was prepared in the manner of Example 1 with the following modifications: Substituting 5-(p-cyanophenyl)-4-pentynoic acid for 5-(p-cyanophenyl)pentanoic acid and 3-methyl-beta-alanine for 3-phenyl-beta-alanine in procedure C of Example 1. The product was verified by C NMR (CD3OD) delta 15.5, 20.3, 34.5, 40.8, 42.0, 80.3, 92.2, 126.1, 127.8 131.2, 133.5, 166.7, 169.7, 172.5.

出典と根拠

ORDレコード
ord-7f66270e73614284b8d1b3a600201844
出典データセット
uspto-grants-1993_06
特許番号
US05220050

反応ノート

読み込み中…