Hexanoic acid, 2-bromo-, methyl ester → HCID 13706743、化合物
反応式
Br[CH:2]([CH2:7][CH2:8][CH2:9][CH3:10])[C:3]([O:5][CH3:6])=[O:4].[F-:11].[K+]>C(N)(=O)C>[F:11][CH:2]([CH2:7][CH2:8][CH2:9][CH3:10])[C:3]([O:5][CH3:6])=[O:4]参加物
4
反応条件
- 温度
- 105 °C
実験手順
Methyl 2-bromocaproate (40 g) was added to anhydrous potassium fluoride (23 g) in acetamide (23 g) kept at 105° C. The mixture was vigorously stirred at 105° C. for 6 hours. The crude product obtained after the conventional work-up was distilled. Yield; 20 g (71 %), b.p.; 66° C./20 mmHg
後処理
- customkept at 105° C
出典と根拠
- ORDレコード
- ord-29a8566348004da5a9a02deef3027dfa
- 出典データセット
- uspto-grants-1993_06
- 特許番号
- US05221763
反応ノート
読み込み中…