4-(3,5-Dimethoxyphenyl)-1-(phenylmethyl)-2-piperazinecarboxamide → 4-(3,5-Dimethoxyphenyl)-1-(phenylmethyl)-2-piperazinemethanamine
反応式
[CH3:1][O:2][C:3]1[CH:4]=[C:5]([N:11]2[CH2:16][CH2:15][N:14]([CH2:17][C:18]3[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=3)[CH:13]([C:24]([NH2:26])=O)[CH2:12]2)[CH:6]=[C:7]([O:9][CH3:10])[CH:8]=1.[H-].[Al+3].[Li+].[H-].[H-].[H-]>>[CH3:10][O:9][C:7]1[CH:6]=[C:5]([N:11]2[CH2:16][CH2:15][N:14]([CH2:17][C:18]3[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=3)[CH:13]([CH2:24][NH2:26])[CH2:12]2)[CH:4]=[C:3]([O:2][CH3:1])[CH:8]=1参加物
3
実験手順
In a manner similar to Preparation 2, react 4-(3,5-dimethoxyphenyl)-1-(phenylmethyl)-2-piperazinecarboxamide with lithium aluminum hydride to obtain the title compound.
後処理
- customIn a manner similar to Preparation 2
出典と根拠
- ORDレコード
- ord-4d53fc5fc23048c392116b10bf496bca
- 出典データセット
- uspto-grants-1993_06