Hydrogen Peroxide → 6-Carbamoyl-1-(1-imidazolyl)-3,4-dihydronaphthalene
反応式
C(=O)([O-])[O-:2].[K+].[K+].OO.[C:9]([C:11]1[CH:12]=[C:13]2[C:18](=[CH:19][CH:20]=1)[C:17]([N:21]1[CH:25]=[CH:24][N:23]=[CH:22]1)=[CH:16][CH2:15][CH2:14]2)#[N:10].O>CS(C)=O.C(Cl)Cl>[C:9]([C:11]1[CH:12]=[C:13]2[C:18](=[CH:19][CH:20]=1)[C:17]([N:21]1[CH:25]=[CH:24][N:23]=[CH:22]1)=[CH:16][CH2:15][CH2:14]2)(=[O:2])[NH2:10]参加物
7
実験手順
Potassium carbonate and 30% aqueous H2O2 solution are added several times, within a period of 24 hours, to 6-cyano-1-(1-imidazolyl)-3,4-dihydronaphthalene (Example 1) in DMSO and CH2Cl2. Finally, water is added and the solid is filtered off, yielding the title compound.
後処理
- filtrationthe solid is filtered off
出典と根拠
- ORDレコード
- ord-1efc13136af34c82890a9eb275e816b3
- 出典データセット
- uspto-grants-1993_04
- 特許番号
- US05206256
反応ノート
読み込み中…