Methylamine → HCID 178484937、化合物
反応式
[C:1]([NH:3][C:4](=[N:7][CH2:8][C:9]1[CH:14]=[CH:13][C:12]([CH2:15][CH2:16][OH:17])=[CH:11][CH:10]=1)SC)#[N:2].[CH3:18][NH2:19]>CO>[C:1]([NH:3][C:4]([NH:19][CH3:18])=[N:7][CH2:8][C:9]1[CH:14]=[CH:13][C:12]([CH2:15][CH2:16][OH:17])=[CH:11][CH:10]=1)#[N:2]参加物
4
実験手順
A solution of 0.42 g (0.00168 mol) of N-cyano-N'-[4-(2-hydroxyethyl)benzyl]-S-methylisothiourea in 50 ml of methanol and 10 g of methylamine was stirred at room temperature overnight. Evaporation of the solvent gave the title compound.
後処理
- customEvaporation of the solvent
出典と根拠
- ORDレコード
- ord-5cce1d8a132e42e2ad6483d450446a82
- 出典データセット
- uspto-grants-1993_04
- 特許番号
- US05206240
反応ノート
読み込み中…