反応式
[Br:1]Br.[O:3]=[C:4]1[C:9]([C:10]#[N:11])=[CH:8][CH:7]=[CH:6][NH:5]1>C(O)(=O)C>[Br:1][C:7]1[CH:8]=[C:9]([C:10]#[N:11])[C:4](=[O:3])[NH:5][CH:6]=1参加物
4
実験手順
Bromine (29 ml, 560 mmol) was added to a stirred solution of 2-oxo-1,2-dihydro-pyridine-3-carbonitrile (34 g, 280 mmol) in acetic acid (180 ml) at room temperature. After 14 hours the reaction mixture was concentrated in vacuo and the resulting oil was trituated with ethanol to afford the title compound as a solid.
後処理
- concentrationAfter 14 hours the reaction mixture was concentrated in vacuo
出典と根拠
- ORDレコード
- ord-bad87c6cf601468b882f553d00f8474a
- 出典データセット
- uspto-grants-2007_11
- 特許番号
- US07297792B2
関連ノート
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