1-Bromo-3-isopropoxybenzene → 2-(Propan-2-yloxy)benzaldehyde
反応式
[CH:1]([O:4][C:5]1[CH:10]=[CH:9][CH:8]=[CH:7][C:6]=1Br)([CH3:3])[CH3:2].BrC1C=CC=[C:15]([O:19]C(C)C)C=1>>[CH:1]([O:4][C:5]1[CH:10]=[CH:9][CH:8]=[CH:7][C:6]=1[CH:15]=[O:19])([CH3:3])[CH3:2]参加物
3
実験手順
The title compound was prepared as in Example 257A but employing 2-iso-propyloxybromobenzene in lieu of 1-bromo-3-isopropoxybenzene. Purification on silica, gel with 10% ether/hexane afforded the title compound (2.3 g, 70%).
後処理
- customThe title compound was prepared as in Example 257A
- customPurification on silica, gel with 10% ether/hexane
出典と根拠
- ORDレコード
- ord-2da7e06ccd1c47028a00ce179b1128be
- 出典データセット
- uspto-grants-2001_09
- 特許番号
- US06284796B1
反応ノート
読み込み中…