Dimethylformamide → 4-(2-(Dimethylamino)ethyl)benzaldehyde
反応式
Br[C:2]1[CH:7]=[CH:6][C:5]([CH2:8][CH2:9][N:10]([CH3:12])[CH3:11])=[CH:4][CH:3]=1.[Mg].CN([CH:17]=[O:18])C>>[CH3:11][N:10]([CH3:12])[CH2:9][CH2:8][C:5]1[CH:6]=[CH:7][C:2]([CH:17]=[O:18])=[CH:3][CH:4]=1参加物
4
実験手順
2-(4-Bromophenyl)-N,N-dimethylethylamine (6.8 g) was refluxed under heating with magnesium for 1 hr to prepare a Grignard reagent, which was reacted with DMF to give the objective 4-(2-dimethylaminoethyl)benzaldehyde as an oil (4.2 g).
出典と根拠
- ORDレコード
- ord-3829d2f2230f418abd08f4b1fb067420
- 出典データセット
- uspto-grants-2001_09
- 特許番号
- US06288061B1
反応ノート
読み込み中…