Formic Acid → 3-Formylaminophenol
反応式
[NH2:1][C:2]1[CH:3]=[C:4]([OH:8])[CH:5]=[CH:6][CH:7]=1.[CH:9](O)=[O:10]>>[CH:9]([NH:1][C:2]1[CH:3]=[C:4]([OH:8])[CH:5]=[CH:6][CH:7]=1)=[O:10]参加物
3
実験手順
A mixture of 100 g m-aminophenol and 150 g formic acid was refluxed for 1.5 h and then evaporated to dryness under reduced pressure (90°-95° C., 10-15 mm Hg). Solid material was dried at 100° C., 10 mm Hg, for 1.5 h. 117 g of the title compound were isolated, melting point 112° C.
後処理
- temperaturewas refluxed for 1.5 h
- customevaporated to dryness under reduced pressure (90°-95° C., 10-15 mm Hg)
- customSolid material was dried at 100° C.
出典と根拠
- ORDレコード
- ord-bc624360872240eab7104b564913aeef
- 出典データセット
- uspto-grants-1998_04
- 特許番号
- US05739318
反応ノート
読み込み中…