Chromium oxide → Bismuth oxide antimony oxide chromium oxide boron oxide

HRID 1599353

反応式

HRID 1599353 の反応式
[Bi:1]=[O:2].[Sb:3]=[O:4].[O-2:5].[Cr+3:6].[O-2].[O-2].[Cr+3].[B:10]=O>>[Bi:1]=[O:2].[Sb:3]=[O:4].[O-2:2].[Cr+3:6].[O-2:2].[O-2:2].[Cr+3:6].[B:10]=[O:5]

参加物

5

実験手順

A bismuth oxide powder (whose average particle size is about 2 to 3 μm) and an antimony oxide powder (whose average particle size is about 2 to 3 μm) were mixed at a weight ratio of 85:15. The blended powder was heat treated at a temperature of 550° C. for 5 hrs. in the air. Further, bismuth oxide fine particles (whose average particle size is about 2 to 3 μm) and a chromium oxide fine powder (whose average particle size is about 0.5 to 1.5 μm) were mixed at a weight ratio of 75:25. The mixed powder was heat treated at a temperature of 600° C. for 10 min. in the air. A bismuth oxide powder (whose average particle size is about 2 to 3 μm) and a boron oxide fine powder (whose average particle size is about 2 to 3 μm) were mixed at a weight ratio of 93:7. The mixed powder was heat treated at a temperature of 600° C. for 10 min. in the air. These were mixed at a weight ratio of 3.0:0.3:0.3 and ground fine for 18 hrs. by means of stabilizing zirconia balls in a monomalon pot. Consequently, a synthetic powder of bismuth oxide/antimony oxide/chromium oxide/boron oxide synthetic powder (whose average particle size is about 2 to 3 μm) was obtained.

後処理

  1. temperatureThe blended powder was heat
  2. additiontreated at a temperature of 550° C. for 5 hrs
  3. temperatureThe mixed powder was heat
  4. additiontreated at a temperature of 600° C. for 10 min. in the air
  5. temperatureThe mixed powder was heat
  6. additiontreated at a temperature of 600° C. for 10 min. in the air
  7. additionThese were mixed at a weight ratio of 3.0:0.3:0.3

出典と根拠

ORDレコード
ord-372fcc3dd8dd4f2db1daaec2e7446a65
出典データセット
uspto-grants-1998_04
特許番号
US05739742

関連ノート

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