1,3-Bis(aminomethyl)cyclohexane → 1,3-Benzenedimethanamine
反応式
[NH2:1][CH2:2][CH:3]1[CH2:8][CH2:7][CH2:6][CH:5]([CH2:9][NH2:10])[CH2:4]1>C1(C)C=CC=C(C)C=1>[NH2:1][CH2:2][CH:3]1[CH2:8][CH2:7][CH2:6][CH:5]([CH3:9])[CH2:4]1.[CH3:9][C:5]1[CH:4]=[C:3]([CH:8]=[CH:7][CH:6]=1)[CH2:2][NH2:1].[C:5]1([CH2:9][NH2:10])[CH:6]=[CH:7][CH:8]=[C:3]([CH2:2][NH2:1])[CH:4]=1参加物
5
実験手順
As a result of analysis by gaschromatography, it was found that the yield of 1,3-bis(aminomethyl)cyclohexane was 93,1 mol %, and as other products 0.1 mol % of metaxylene, 6.1 mol % of 3-aminomethyl-1-methylcyclohexane, 0.2 mol % of 3-methylbenzylamine and 0.2 mol % of unreacted metaxylylenediamine were obtained.
後処理
- customAs a result of analysis by gaschromatography, it
出典と根拠
- ORDレコード
- ord-38a1f91225a6484998938dd99ddaeafc
- 出典データセット
- uspto-grants-1998_04
- 特許番号
- US05741928
反応ノート
読み込み中…