[6-(2,2,3,3-Tetrafluoropropoxy)pyridin-3-yl]methanol → 6-(2,2,3,3-Tetrafluoropropoxy)nicotinaldehyde
反応式
[F:1][C:2]([F:16])([CH:13]([F:15])[F:14])[CH2:3][O:4][C:5]1[CH:10]=[CH:9][C:8]([CH2:11][OH:12])=[CH:7][N:6]=1>[O-2].[O-2].[Mn+4]>[F:16][C:2]([F:1])([CH:13]([F:15])[F:14])[CH2:3][O:4][C:5]1[CH:10]=[CH:9][C:8]([CH:11]=[O:12])=[CH:7][N:6]=1参加物
3
実験手順
2-(2,2,3,3-Tetrafluoropropoxy)-5-(hydroxymethyl)pyridine was treated with active manganese dioxide in the same manner as in Reference example 22 to obtain the title compound as an oil in a yield of 96%.
出典と根拠
- ORDレコード
- ord-d29ccb5c55604be19a452e6db5fe80cd
- 出典データセット
- uspto-grants-1999_11
- 特許番号
- US05977152
反応ノート
読み込み中…