3-(3,4-Dichlorophenoxy)benzaldehyde → HCID 18394922、化合物

HRID 1602958

反応式

HRID 1602958 の反応式
[CH3:1][C:2]([Si:5]([CH3:38])([CH3:37])[O:6][C@@H:7]1[C@H:11]([O:12][Si:13]([C:16]([CH3:19])([CH3:18])[CH3:17])([CH3:15])[CH3:14])[C@@H:10]([CH2:20][O:21][Si:22]([C:25]([CH3:28])([CH3:27])[CH3:26])([CH3:24])[CH3:23])[O:9][C@H:8]1[N:29]1[CH:36]=[CH:35][C:33](=[O:34])[NH:32][C:30]1=[O:31])([CH3:4])[CH3:3].[Cl:39][C:40]1[CH:41]=[C:42]([CH:52]=[CH:53][C:54]=1[Cl:55])[O:43][C:44]1[CH:45]=[C:46]([CH:49]=[CH:50][CH:51]=1)[CH:47]=[O:48]>>[Cl:39][C:40]1[CH:41]=[C:42]([CH:52]=[CH:53][C:54]=1[Cl:55])[O:43][C:44]1[CH:45]=[C:46]([CH:47]([OH:48])[C:35]2[C:33](=[O:34])[NH:32][C:30](=[O:31])[N:29]([CH:36]=2)[C@@H:8]2[O:9][C@H:10]([CH2:20][O:21][Si:22]([C:25]([CH3:26])([CH3:27])[CH3:28])([CH3:23])[CH3:24])[C@@H:11]([O:12][Si:13]([C:16]([CH3:17])([CH3:18])[CH3:19])([CH3:14])[CH3:15])[C@H:7]2[O:6][Si:5]([C:2]([CH3:1])([CH3:3])[CH3:4])([CH3:38])[CH3:37])[CH:49]=[CH:50][CH:51]=1

参加物

3

反応物 2

HCID 1572893-(3,4-Dichlorophenoxy)benzaldehydeHCID 10841090HCID 10841090、化合物

生成物 1

HCID 18394922HCID 18394922、化合物

実験手順

5-((3-(3,4-Dichlorophenoxy)phenyl)hydroxymethyl)-2',3',5'-tris-O-((1,1-dimethylethyl)dimethylsilyl)uridine was prepared from 2',3',5'-tris-O-((1,1-dimethylethyl)dimethylsilyl)uridine according to the method of Example 1 step (i) (using 3-(3,4-dichlorophenoxy)benzaldehyde instead of benzophenone) as a colourless foam.

出典と根拠

ORDレコード
ord-70c6b7f54c5847feb0b280646aba5630
出典データセット
uspto-grants-1999_11
特許番号
US05985849

関連ノート

読み込み中…