化工社化工社 化学情報印刷レポート · 研究参考用
Hexamethylcyclotrisiloxane → Nonamethyltetrasiloxanyl 2-methylprop-2-enoate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Hexamethylcyclotrisiloxane | HCID 10914 | — |
| 反応物 | Trifluoromethanesulfonic acid | HCID 62406 | — |
| 反応物 | 2-Propenoic acid, 2-methyl-, trimethylsilyl ester | HCID 2733839 | — |
| 溶媒 | Triethylamine | HCID 8471 | — |
| 生成物 | Nonamethyltetrasiloxanyl 2-methylprop-2-enoate | HCID 12991985 | — |
反応手順
5 g of hexamethylcyclotrisiloxane, 3.5 g of trimethylsilyl methacrylate, 0.016 g of trifluoromethane sulfonic acid were stirred for 24 h at room temperature. 0.5 ml of triethylamine was then added, and the salts were filtered to furnish nonamethyl-1-methacryloyloxy-tetrasiloxane.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07736634B2 |
| 出典データセット | uspto-grants-2010_06 |
| ORD ID | ord-489fa28b7e0444db86d097bede757586 |
| 出典メモ | uspto-grants-2010_06 |