化工社化工社 化学情報印刷レポート · 研究参考用
Toluene → Nonamethyltetrasiloxanyl 2-methylprop-2-enoate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Toluene | HCID 1140 | — |
| 反応物 | Hexamethylcyclotrisiloxane | HCID 10914 | — |
| 反応物 | 2-Propenoic acid, 2-methyl-, trimethylsilyl ester | HCID 2733839 | — |
| 生成物 | Nonamethyltetrasiloxanyl 2-methylprop-2-enoate | HCID 12991985 | — |
反応手順
5 g of hexamethylcyclotrisiloxane, 3.5 g of trimethylsilyl methacrylate and 0.3 g of Amberlyst A15 resin catalyst were stirred in 2.5 ml of toluene. After 7 h at room temperature the catalyst was filtered and the solvent evaporated under reduced pressure to furnish nonamethyl-1-methacryloyloxy-tetrasiloxane.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07736634B2 |
| 出典データセット | uspto-grants-2010_06 |
| ORD ID | ord-8709a273d055413f9e38955d2fe3c86e |
| 出典メモ | uspto-grants-2010_06 |