Hydrochloric Acid → 2-methoxy-N-methyl-3-morpholino-2-(2-pyridyl)thiopropanamide hydrochloride
反応式
[CH3:1][O:2][C:3]([C:15]1[CH:20]=[CH:19][CH:18]=[CH:17][N:16]=1)([CH2:8][N:9]1[CH2:14][CH2:13][O:12][CH2:11][CH2:10]1)[C:4]([NH:6][CH3:7])=[S:5].[ClH:21]>CCOCC>[ClH:21].[CH3:1][O:2][C:3]([C:15]1[CH:20]=[CH:19][CH:18]=[CH:17][N:16]=1)([CH2:8][N:9]1[CH2:10][CH2:11][O:12][CH2:13][CH2:14]1)[C:4]([NH:6][CH3:7])=[S:5]参加物
4
実験手順
One gram of 2-methoxy-N-methyl-3-morpholino-2-(2-pyridyl)thiopropanamide in ether is added to ethereal hydrogen chloride. The resulting precipitate is filtered off and recrystallized from ethanol/ether to give 2-methoxy-N-methyl-3-morpholino-2-(2-pyridyl)thiopropanamide hydrochloride.
後処理
- filtrationThe resulting precipitate is filtered off
- customrecrystallized from ethanol/ether
出典と根拠
- ORDレコード
- ord-83068ae0e12643a7893f4141c0ec8210
- 出典データセット
- uspto-grants-1976_04
- 特許番号
- US03948892
反応ノート
読み込み中…