Benzaldehyde → HCID 474291、化合物
反応式
[CH:1](=O)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[SH:9][CH:10]([CH2:13][SH:14])[CH2:11][OH:12]>>[OH:12][CH2:11][CH:10]1[CH2:13][S:14][CH:1]([C:2]2[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=2)[S:9]1参加物
3
実験手順
According to the procedure of Example 1, 35 g. (0.33 mole) of benzaldehyde and 40 g. (0.33 mole) of 2,3-dimercaptopropanol were reacted to yield 63.6 g. of crude product. After recrystallization 42.4 (56%) of the desired product were obtained as shown by nmr spectroscopy.
後処理
- customto yield 63.6 g
- customAfter recrystallization 42.4 (56%) of the desired product
- customwere obtained
出典と根拠
- ORDレコード
- ord-06d67170767d42f799eb27100edd6b5c
- 出典データセット
- uspto-grants-1976_04
- 特許番号
- US03948944
反応ノート
読み込み中…