Boron tribromide → Phenol, 4-(2,2-difluorocyclopropyl)-

反応式

[F:1][C:2]1([F:13])[CH2:4][CH:3]1[C:5]1[CH:10]=[CH:9][C:8]([O:11]C)=[CH:7][CH:6]=1.B(Br)(Br)Br>>[F:1][C:2]1([F:13])[CH2:4][CH:3]1[C:5]1[CH:10]=[CH:9][C:8]([OH:11])=[CH:7][CH:6]=1

参加物

反応物 2

HCID 25134Boron tribromide

HCID 21549152HCID 21549152、化合物

生成物 1

HCID 21549151Phenol, 4-(2,2-difluorocyclopropyl)-

実験手順

p-(2,2-Difluorocyclopropyl)phenol was prepared from 120 g. of p-(2,2-difluorocyclopropyl)anisole and 81 g. of boron tribromide according to the procedure described above in Example 1, part (c), affording 72 g. of oil used directly in the following reaction.

後処理

customaffording 72 g
customof oil used directly in the following reaction

出典と根拠

ORDレコード: ord-9760bec5e0814e4fb5ceb31c1e14c843
出典データセット: uspto-grants-1976_04
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US03948973

反応ノート

読み込み中…

参加物