Methyl Isocyanate → N-Methyl-N'-[2-((5-methyl-4-imidazolyl)methylamino)ethyl]urea
反応式
[CH3:1][C:2]1[NH:6][CH:5]=[N:4][C:3]=1[CH2:7][NH:8][CH2:9][CH2:10][NH2:11].[CH3:12][N:13]=[C:14]=[O:15]>>[CH3:12][NH:13][C:14]([NH:11][CH2:10][CH2:9][NH:8][CH2:7][C:3]1[N:4]=[CH:5][NH:6][C:2]=1[CH3:1])=[O:15]参加物
3
実験手順
By the procedure of Example 24, N-(5-methyl-4-imidazolylmethyl)ethylenediamine is reacted with methyl isocyanate to give, after concentrating and separating the residue by column chromatography, the title compound.
後処理
- customto give
- concentrationafter concentrating
- customseparating the residue by column chromatography
出典と根拠
- ORDレコード
- ord-cd2f1f3ba3704d238b07bcea99a46099
- 出典データセット
- uspto-grants-1976_04
- 特許番号
- US03950353
反応ノート
読み込み中…