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Peracetic Acid → 4-Tert-octylcatechol
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Peracetic Acid | HCID 6585 | — |
| 反応物 | 4-Tert-octylphenol | HCID 8814 | — |
| 反応物 | Perpropionic acid | HCID 65136 | — |
| 溶媒 | Acetone | HCID 180 | — |
| 生成物 | 4-Tert-octylcatechol | HCID 70828 | 61% |
反応手順
The procedure of Example 8 was followed, except 20 ml of acetone was added as a solvent for para-tert.-octyl phenol and 4.5g (0.05 mol) of perpropionic acid in the form of about 25 weight% acetone solution was added over 20 minutes in place of peracetic acid. Consequently, the conversion of para-tert.-octyl phenol was 6.8%, 4-tert.-octyl pyrocatechol was formed in a yield of 61% based on the converted octyl phenol and the conversion of perpropionic acid was 100%.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US03950437 |
| 出典データセット | uspto-grants-1976_04 |
| ORD ID | ord-021a4408e9c9420987461663e7b55917 |
| 出典メモ | uspto-grants-1976_04 |