Hexadec-1-ene-1-sulfonic acid → 1-Hexadecene

HRID 1605806ノート

反応式

HRID 1605806 の反応式
[CH:1](S(O)(=O)=O)=[CH:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH3:16]>CC(C)=O>[CH2:1]=[CH:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH3:16]

参加物

3

反応物 1

HCID 107566Hexadec-1-ene-1-sulfonic acid

生成物 1

HCID 123951-Hexadecene

試薬・触媒・溶媒 1

HCID 180Acetone溶媒

実験手順

The aqueous-acetone layer which contained the sulfonic acid fraction of the product was stripped of solvents at 40°-45°C. under a vacuum to give 2.85 g. of viscous acid identified as hexadecene sulfonic acid on the basis of an IR spectrum which showed the presence of trans olefinic double bond (965 cm-1) and the absence of sultones (no 830 and 530 cm-1 bands).

後処理

  1. customwas stripped of solvents at 40°-45°C. under a vacuum
  2. customto give 2.85 g

出典と根拠

ORDレコード
ord-47b3cf032cd04a88af3fdbac6b14dce9
出典データセット
uspto-grants-1976_04
特許番号
US03951823

反応ノート

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