2,5-Dibenzyl-2,5-diazabicyclo[2.2.2]octane-3,6-dione → 2,5-Dibenzyl-2,5-diazabicyclo[2.2.2]octane
反応式
[CH2:1]([N:8]1[C:13](=O)[CH:12]2[CH2:15][CH2:16][CH:9]1[C:10](=O)[N:11]2[CH2:17][C:18]1[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=1)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.C(N1C2CCC1CN(C)C2)C1C=CC=CC=1>>[CH2:1]([N:8]1[CH2:13][CH:12]2[CH2:15][CH2:16][CH:9]1[CH2:10][N:11]2[CH2:17][C:18]1[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=1)[C:2]1[CH:3]=[CH:4][CH:5]=[CH:6][CH:7]=1参加物
3
実験手順
Reduction of 6.1 g (0.019 mole) of 2.5-dibenzyl-2,5-diazabicyclo[2.2.2]octane-3,6-dione by the procedure employed to prepare 8-benzyl-3-methyl-3,8-diazabicyclo[3.2.1]octane as related under Example 5 gave 4.9 g (88%) of 2,5-dibenzyl-2,5-diazabicyclo[2.2.2]octane as a colorless oil.
出典と根拠
- ORDレコード
- ord-935699de279a40c485bc3c5a131dc5de
- 出典データセット
- uspto-grants-1976_04