Triethylamine → 1175-97-9
反応式
[CH3:1][C:2]1([CH3:24])[S:6][C@@H:5]2[C@H:7]([NH:10][C:11]([C@H:13]([NH2:20])[C:14]3[CH:15]=[CH:16][CH:17]=[CH:18][CH:19]=3)=[O:12])[C:8](=[O:9])[N:4]2[C@H:3]1[C:21]([OH:23])=[O:22].O.O.O.S([O-])([O-])(=O)=O.[Mg+2].[CH2:34]([N:36]([CH2:39][CH3:40])[CH2:37][CH3:38])[CH3:35]>ClCCl>[CH3:1][C:2]1([CH3:24])[S:6][C@@H:5]2[C@H:7]([NH:10][C:11]([C@H:13]([NH2:20])[C:14]3[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=3)=[O:12])[C:8](=[O:9])[N:4]2[C@H:3]1[C:21]([OH:23])=[O:22].[CH2:34]([N:36]([CH2:39][CH3:40])[CH2:37][CH3:38])[CH3:35]参加物
5
実験手順
After stirring a mixture of 806 mg. of ampicillin trihydrate, 600 mg. of magnesium sulfate, 0.42 ml. of triethylamine, and 14 ml. of dichloromethane for 1 hour at room temperature, magnesium sulfate was fitered off to provide a dichloromethane solution of ampicillin triethylamine salt.