Hydrate;hydrochloride → HCID 178419078、化合物

HRID 1607315ノート

反応式

HRID 1607315 の反応式
Cl.O.[NH2:3][CH:4]([C:11]([OH:13])=[O:12])[CH2:5][C:6]1[N:10]=[CH:9][NH:8][CH:7]=1.Cl.O>O>[NH2:3][C@H:4]([C:11]([OH:13])=[O:12])[CH2:5][C:6]1[N:10]=[CH:9][NH:8][CH:7]=1

参加物

4

反応物 2

HCID 21885828Hydrate;hydrochlorideHCID 178479203HCID 178479203、化合物

生成物 1

HCID 178419078HCID 178419078、化合物

試薬・触媒・溶媒 1

HCID 962Water溶媒

実験手順

HCl.H2O: D,L-His.HCl.H2O (3.2 g) and the appropriate polymer were slurried in water (5 ml) and the slurry was heated to complete dissolution. The hot solution was filtered and allowed to stand at 50° C. for 20 hrs without agitation. The crystals were collected by filtration and the enantiomeric excess was determined. The results are summarized in Table VI.

後処理

  1. temperaturethe slurry was heated
  2. dissolutiondissolution
  3. filtrationThe hot solution was filtered
  4. filtrationThe crystals were collected by filtration

出典と根拠

ORDレコード
ord-65c5551bfb56438f89c3c7abed1f1c95
出典データセット
uspto-grants-1989_09
特許番号
US04864031

反応ノート

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