Acetaldehyde → Quindoxin

HRID 1607718

反応式

HRID 1607718 の反応式
[CH:1]1[CH:9]=[CH:8][C:7]2[C:3](=[N:4][O:5][N+:6]=2[O-:10])[CH:2]=1.[CH:11](=O)[CH3:12]>C(N(CC)CC)C>[CH:9]1[CH:8]=[C:7]2[N:6]([O-:10])[CH:11]=[CH:12][N+:4](=[O:5])[C:3]2=[CH:2][CH:1]=1

参加物

4

反応物 2

HCID 177AcetaldehydeHCID 68075Benzofuroxan

生成物 1

HCID 72073Quindoxin

試薬・触媒・溶媒 1

HCID 8471Triethylamine溶媒

実験手順

A mixture of benzofuroxan (2.5 g.), acetaldehyde (2.5 ml.) and triethylamine (20 ml.) is allowed to stand at room temperature for 24 hours. The solid material which precipitates is filtered and dried to give product, M.P. 223°-224° C. dec. (MIC against P. vulgaris is 12.5 mcg./ml.).

後処理

  1. customThe solid material which precipitates
  2. filtrationis filtered
  3. customdried
  4. customto give product, M.P. 223°-224° C. dec. (MIC against P. vulgaris is 12.5 mcg./ml.)

出典と根拠

ORDレコード
ord-8ce7d3dd4f95463ab3b62df2f02df71b
出典データセット
uspto-grants-1989_09
特許番号
US04866175

関連ノート

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