関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | m-Chloroperbenzoic acid | HCID 70297 | — |
| 反応物 | 4-(4-Pentenoxy)-4'-nitrobiphenyl | HCID 19901284 | — |
| 溶媒 | Dichloromethane | HCID 6344 | — |
| 生成物 | 4-(4,5-Epoxypentoxy)-4'-nitrobiphenyl | HCID 22163019 | — |
反応手順
To 250 ml of methylene chloride is added 28.3 g of 4-(4-penteneoxy)-4'-nitrobiphenyl. The solution is cooled to 0° C.,and 18 g of meta-chloroperbenzoic acid is added slowly. The mixture is stirred at 0° C. for 24 hours, and allowed to warm to room temperature.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US04867538 |
|---|
| 出典データセット | uspto-grants-1989_09 |
|---|
| ORD ID | ord-0512e8fd2ffb448cb418893863e87e58 |
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| 出典メモ | uspto-grants-1989_09 |
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