化工社化工社 化学情報印刷レポート · 研究参考用
Ethanol → Butyric acid (4-quinolinylmethylene)hydrazide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Ethanol | HCID 702 | — |
| 反応物 | Butyrohydrazide | HCID 77079 | — |
| 反応物 | 4-Quinolinecarboxaldehyde | HCID 78072 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | Butyric acid (4-quinolinylmethylene)hydrazide | HCID 86743403 | 85.4% |
反応手順
A mixture of 7.85 gm (0.05 mole) of 4-quinolinecarboxaldehyde, 5.11 gm (0.05 mole) of butyric acid hydrazide and 100 ml of ethanol is refluxed 4 hr. The reaction mixture is diluted with water and cooled to room temperature. The mixture is chilled. The solid that separates is collected, washed with water and dried to give 10.3 gm of the title compound, having a melting point of 130.4° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04870082 |
| 出典データセット | uspto-grants-1989_09 |
| ORD ID | ord-86b41a2e023d46cfa519dc8f0d867f61 |
| 出典メモ | uspto-grants-1989_09 |