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HRID 1608175作成日:2026年10月27日

Ethanol → Butyric acid (4-quinolinylmethylene)hydrazide

https://huagongshe.com/reaction/1608175

反応式

関与物質

役割名称HCID仕込み量
反応物EthanolHCID 702—
反応物ButyrohydrazideHCID 77079—
反応物4-QuinolinecarboxaldehydeHCID 78072—
溶媒WaterHCID 962—
生成物Butyric acid (4-quinolinylmethylene)hydrazideHCID 8674340385.4%

反応手順

A mixture of 7.85 gm (0.05 mole) of 4-quinolinecarboxaldehyde, 5.11 gm (0.05 mole) of butyric acid hydrazide and 100 ml of ethanol is refluxed 4 hr. The reaction mixture is diluted with water and cooled to room temperature. The mixture is chilled. The solid that separates is collected, washed with water and dried to give 10.3 gm of the title compound, having a melting point of 130.4° C.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US04870082
出典データセットuspto-grants-1989_09
ORD IDord-86b41a2e023d46cfa519dc8f0d867f61
出典メモuspto-grants-1989_09